Well I am glad I am not the only one! But of course, no sooner than I panicked than it cleared itself again. The pH was pretty low this morning, so I added bicarb to get it back up (no time for a water change before work), and the nitrite must have processed well over 5ppm in a little less than 12 hours. So I am not going to water change for now, but hope that the 'spike' is over and we are back on the right track...
Thanks Taffy, for the interpretation of the results - it is good to know in advance that pH swings are possible, and something to look out for. That said, ever since I started proper regular testing on my small tank, the pH has been absolutely steady at 7.4 - not a blip. That said, it has also been consistent double zeros, so had I been testing back when I was doing a fish-in cycle (when I knew nothing about it at all, sorry fishies
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) it may have been a bit more dramatic.
On a not so good note, my ramblings about my new tank convinced my office room-mate that she wanted to get another tanks after having none at all for a couple of years. I told her about fishless cycling and sent a link to this site, but only two days after her new tank (maybe 60 or 70 litres by the sound of it?) had been sat running on the cabinet, her son came home with two platties, two guppies and two juvenile angels. I have tried prompting water tests, but I think it is falling on deaf ears. Maybe when they have two angels, 197 platties and 3,492 guppies I will have to rescue the angels...